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Beilstein J. Org. Chem. 2018, 14, 1655–1659, doi:10.3762/bjoc.14.141
Graphical Abstract
Scheme 1: Synthesis of THP ether 3a.
Scheme 2: Synthesis of THP ethers 3b–l in the presence of NH4HSO4@SiO2. All reactions were run at rt, in the ...
Scheme 3: Deprotection of THP ether 3i.
Scheme 4: One-pot synthesis of 3-[4-(tetrahydro-2H-pyran-2-yl)oxymethylphenyl]-3-pentanol (4fa).
Scheme 5: One-pot synthesis of 4-(tetrahydro-2H-pyran-2-yloxymethyl)benzyl alcohol (4fb).